This method is for the collection and analysis of 1,1,1-trichloroethane. The sample is collected on charcoal adsorbent, desorbed with carbon disulfide, and analyzed by GC/FID.
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| Hold Times, Preservatives, Preps, Collection, Analytical & Documentation | |
|---|---|
| Holding Time: | The recovery of the analyte from the collection medium after storage must be 75% or greater. Recoveries of greater than 100% were obtained from samples stored for up to 15 days at both ambient (18.2 - 21°C) and refrigerated (-4 - 3°C) temperatures. |
| Preservatives: | Not noted in method |
| Required Preps: | Solid sorbent tubes: coconut shell charcoal, 100 mg/50 mg, 7cm x 6mm OD x 4mm ID |
| Collection Method: | Solid sorbent tubes: 3 L at 0.2 L/min. |
| Analytical Methodology: | GC/FID |
| Documentation: | 
014
|
| Analyte | Formula | CAS Number | Detection Limit | |
|---|---|---|---|---|
| 1,1,1-Trichloroethane | C2H3Cl3 |
71-55-6 |
1.2 |
µg |
* The analytes and detection limits listed for each method represent the typical detection limits and analytes reported for that particular method. Keep in mind that analyte lists may vary from laboratory to laboratory. Detection limits may also vary from lab to lab and are dependent upon the sample size, matrix, and any interferences that may be present in the sample.