Method 4

Vinyl chloride by GC/FID


This method is for the determination of vinyl chloride. The sample is collected on charcoal sorbent tubes, desorbed with carbon disulfide, and analyzed by gas chromatography with a flame ionization detector. Sample should be refrigerated and analyzed as soon as possible.


(OSHA)

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Method Data

Hold Times, Preservatives, Preps, Collection, Analytical & Documentation
Holding Time:   Analyze as soon as possible
Preservatives:   Samples must be refrigerated.
Required Preps:   Solid sorbent tubes: coconut shell charcoal, 100mg/50mg, 7cm x 6mm OD x 4mm ID.
Collection Method:   Solid sorbent charcoal tubes; 10 L @ 0.2 L/min.
Analytical Methodology:   GC/FID
Documentation:   004

Analyte List*

Analyte Formula CAS Number Detection Limit
Vinyl chloride
C2H3Cl
75-01-4
0.6
 ng

* The analytes and detection limits listed for each method represent the typical detection limits and analytes reported for that particular method. Keep in mind that analyte lists may vary from laboratory to laboratory. Detection limits may also vary from lab to lab and are dependent upon the sample size, matrix, and any interferences that may be present in the sample.